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Academia | The Offset
http://offset.peczuh.uconn.edu/tag/academia
Posts Tagged ‘Academia’. The Ride of a Lifetime: a Fulbright Experience. Posted by Mark W. Peczuh. Note: This is the long-read version of a post that appeared in the UConn Today. More photos from Barca on flickr. Research Collaboration: Let’s get the proteins to do the work. Life Outside the Lab: Diversions. The Heart of the Matter. In the spirit of the Fulbright program, I arranged interviews with a few scientists in Barcelona whose research interests are similar to mine. Interviews were extracurric...
Synthesis | The Offset
http://offset.peczuh.uconn.edu/tag/synthesis
Posts Tagged ‘Synthesis’. Sympathy for the amide bond. Enantioselective Total Synthesis of (-)-Lansai B and -Nocardioazines A and B. Haoxuan Wang and Sarah E. Reisman. Angew Chem. Int. Ed. 6206-6210 DOI: 10.1002/anie.201402571. Nothing incites apoplexy in your favorite peptide chemist like mentioning how real synthetic chemists are dismissive of the challenges that can arise, from time to time, in the formation of amide bonds. C’mon. How hard can it really be? Reporting the syntheses of (-)-lansai B ( 1.
Diazonamide dot-com | The Offset
http://offset.peczuh.uconn.edu/2016/09/09/diazonamide-dot-com
I was at a conference this summer. Where Patrick Harran gave a lecture on his group’s approach toward the synthesis of callyspongiolide. Diazonamide was a hot target during an interesting time the turn of the century. We were still afloat on the dotcom bubble of the roaring 90’s. And as you well know, that bubble burst. On a much smaller scale (a molecular scale! Nicolaou, a major player in the diazonamide story, even wrote a review. About those examples and some of the emotions that surrounded them....
How VanA Strains Get Away With It, Part Two | The Offset
http://offset.peczuh.uconn.edu/2015/10/08/how-vana-strains-get-away-with-it-part-two
How VanA Strains Get Away With It, Part Two. An evaluation of the thermodynamics of binding between various ligands of Vancomycin (Part 2/2). Part 1 in this series can be found here on The Offset. And also at the Winnower. Vancomycin Molecular Recognition Events (cont’d). Concluded, after extensive investigation, that an amide-amide H-bond in ligated VC is worth 0 to 2 kcal/mol (which agrees with the. Presumably, substitution of a methylene CH. After devising a synthetic strategy to prepare ligand 3.
Sympathy for the amide bond | The Offset
http://offset.peczuh.uconn.edu/2014/09/09/sympathy-for-the-amide-bond
Sympathy for the amide bond. Enantioselective Total Synthesis of (-)-Lansai B and -Nocardioazines A and B. Haoxuan Wang and Sarah E. Reisman. Angew Chem. Int. Ed. 6206-6210 DOI: 10.1002/anie.201402571. Nothing incites apoplexy in your favorite peptide chemist like mentioning how real synthetic chemists are dismissive of the challenges that can arise, from time to time, in the formation of amide bonds. C’mon. How hard can it really be? Activate an acid using your favorite alphabet soup reagent. The strat...
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Peczuh Research Group › University of Connecticut
http://www.peczuh.uconn.edu/about/index.html
The Peczuh Research Group investigates the inter-relationship between structure and function of small molecules in the context of biological activity. Organic synthesis is an integral tool in our research program. We develop new routes to molecules of intermediate complexity to address structure-activity relationships. The Group supports an inclusive research environment that encourages inquiry through rigorous experimentation, sound logic and unconventional thinking. Mark W. Peczuh. Storrs, CT 06269-3060.
Peczuh Research Group › University of Connecticut
http://www.peczuh.uconn.edu/index.php
Peczuh Research Group › University of Connecticut. We are uncovering principles that govern the shape of macrocycles. QM/MM computed complex between ConA and a methyl septanoside. Reaction Discovery: Turning Spiroketals Inside Out. Cava is the only way to celebrate a successful thesis defense. Tweets by @peczuh research. Blog: In the Pipeline. Blog: Master Organic Chemistry. Connect with Peczuh Research Group:.
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A Chocolate Bloom Analogy for Crumbling Concrete in Home Foundations*. Have you ever unwrapped a piece of chocolate only to find it has a whitish powder surrounding it? It almost stops you from eating the chocolate, right? Chocolate that gets the whitish powdery appearance is said to have undergone a bloom called chocolate bloom. Bloomed chocolate is completely edible and tastes almost as good as regular chocolate. Crumbling concrete, on the other hand, is very hard to swallow. November 18, 2016. It was ...
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