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Round Bottom Flask

Follow the trials and tribulations of a bunch of Aussie Chemists as we plow through life in the lab.

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Round Bottom Flask | roundbottomflask.blogspot.com Reviews
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Follow the trials and tribulations of a bunch of Aussie Chemists as we plow through life in the lab.
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posted by labchimp,18 comments,7 comments,posted by organicoverdose,in the meantime,4 comments,15 comments,labels rbf teaches,damn bureaucrats,damn lab monkeys,labels lab life,rant,older posts,subscribe to rbf,posts,atom,all comments,about rbf,wilhelm
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Round Bottom Flask | roundbottomflask.blogspot.com Reviews

https://roundbottomflask.blogspot.com

Follow the trials and tribulations of a bunch of Aussie Chemists as we plow through life in the lab.

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1

Round Bottom Flask: April 2010

http://roundbottomflask.blogspot.com/2010_04_01_archive.html

Apr 30, 2010. RBF Teaches: Drying solvents. So, when you do real chemistry and are able to use a manifold appropriately you can start to look at some genuinely difficult chemistry requiring dry conditions. The dry (or anhydrous) reaction is quite commonplace in synthetic labs and you will most likely come across it in your career, probably very early on. Once again, I suggest reading APOC. The use of activated molecular sieves or some other innocuous dried material (e.g. KOH for TEA) can be place...Begin...

2

Round Bottom Flask: November 2009

http://roundbottomflask.blogspot.com/2009_11_01_archive.html

Nov 30, 2009. RBF Teaches: Column chromatography. Listen up kiddies,. Column chromatography is much the same as TLC. Except this time the solvent front is forced down instead of being drawn up. All of the principles. IMPORTANT NOTE: Silica dust is toxic to inhalation (similar to asbestos) and all measuring of silica should be done in a fume hood and FOR GOD'S SAKES DON'T BREATHE IT IN! Step 1: Choosing the column. This leads us to the important bit: the actual column. So APOC. MSG edit: everyone has thei...

3

Round Bottom Flask: February 2010

http://roundbottomflask.blogspot.com/2010_02_01_archive.html

Feb 26, 2010. MPLC vs Flash Chromatography. Yesterday an old argument reemerged in the lab. On discussing the use of an auto-column and the ways in which we can implement it in the lab and the ways in which time will be saved one of us mentioned that an auto-column MPLC would never be as good as a good ol' hand worked flash column. Image 1) and the Teledyne Combi Flash. Image 2) as well as the Kyle Finchsigmate's MPLC for the people. Image 3). But, are they as good as the good ol' hand column. Reusable c...

4

Round Bottom Flask: Damn bureaucrats! Damn lab monkeys!

http://roundbottomflask.blogspot.com/2010/04/damn-bureaucrats-damn-lab-monkeys.html

Apr 29, 2010. On a chemical side not unrelated, our CEM microwave has failed with a power supply error and the damn thing just came back with a replacement power supply. WTF! I have tried to run some reactions on the damn thing and it fails after 5min. Our water pumps that have lasted for years have all decided to trip all the fumehoods and die all at the same time. We have a brand new MPLC that we can't use and I really want to play with it :P. All in all what a crazy start to this semester. Maybe someo...

5

Round Bottom Flask: December 2009

http://roundbottomflask.blogspot.com/2009_12_01_archive.html

Dec 26, 2009. Season greetings from RBF. Hope you guys had a great christmas. Personally I had one of the better ones this year, and a contributing factor was some pretty neat gifts (which are chemistry related). First up, my gorgeous girlfriend gave me a copy of Julia Child's 'Mastering the art of French cooking'. So there's the link. My second chemistry related christmas gift is this truly stylish. Shirt from the folks at webelements.com. Dec 18, 2009. Came across this on Google Reader this morning:.

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Something Deeply Wrong With Chemistry » Chemistry Blog

http://www.chemistry-blog.com/2010/06/22/something-deeply-wrong-with-chemistry

Laquo; The Good, The Bad, and The Ugly. Art On A Chip. Something Deeply Wrong With Chemistry. An example of what is currently wrong with chemistry culture, even though it is dated. Future chemistry faculty will have to be twice as smart, work with twice the efficiency, and reach the correct positions of influence if they want this type of unhealthy cultural attitudes to finally be put to rest. This is my goal at least. Update 1: Guido Koch now. Update 4: A transcribed letter from Robert Tjian. I realize ...

carbontet.blogspot.com carbontet.blogspot.com

Carbon Tet: CS Support Forum - Safari Problem

http://carbontet.blogspot.com/2010/08/cs-support-forum-safari-problem.html

Musings of an organic chemist. Wednesday, August 25, 2010. CS Support Forum - Safari Problem. Alan Gorman commented in my last post. I should note that the same server problem with the first link occurs in Firefox 3.5.11 as well. When I log in I get a similar error that says the page is not redirecting properly. "Firefox has detected that the server is redirecting the request for this address in a way that will never complete.". Are busted.that doesnt bode well for the future of their operation! Thank yo...

carbontet.blogspot.com carbontet.blogspot.com

Carbon Tet: October 2007

http://carbontet.blogspot.com/2007_10_01_archive.html

Musings of an organic chemist. Thursday, October 25, 2007. Gone but not forgotten. Albert I. Meyers. November 22, 1932 - October 23, 2007. Labels: Albert I. Meyers. Tuesday, October 23, 2007. I think we all need to take the day off and spread the good word about Avogadro. Is anyone else celebrating? Wednesday, October 17, 2007. IBX (not Irritable Bowl Xyndrome). Iwamoto, O. Koshino, H. Hashizume, D. Nagasawa, K., ACIEE, Early View. Friday, October 12, 2007. Al is the MAN! The 2007 Nobel Peace Prize.

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Carbon Tet: Carbon Tetrachloride

http://carbontet.blogspot.com/2010/08/carbon-tetrachloride.html

Musings of an organic chemist. Sunday, August 1, 2010. But this is a chemistry blog, so let's talk a bit more about the molecule. Carbon tet was first prepared way back in 1839. The French chemist Henri Victor Regnault reacted chloroform with chlorine producing carbon tet and HCl. Now it is made from methane but before the 1950s it was prepared by chlorination of carbon disulfide. It could be your hedge against inflation. Welcome back. What have you been up to? Really miss reading your blog.

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Carbon Tet: October 2008

http://carbontet.blogspot.com/2008_10_01_archive.html

Musings of an organic chemist. Thursday, October 9, 2008. A new NIH policy was announced yesterday. And will be applicable to all proposals submitted on or after January 25, 2009. The policy cuts down on the number of times one can resubmit a grant proposal. Currently if a proposal is not funded an amended application can be resubmitted two more times. This policy will restrict all new application and all competing renewal applications to only a single resubmission. Wednesday, October 8, 2008.

chiraljones.wordpress.com chiraljones.wordpress.com

Bigger News | Chiral Jones

https://chiraljones.wordpress.com/2011/01/30/bigger-news

Now with hood space! A little less than a week ago, I received the first acceptance email. After the suspense of a seemingly indefinite wait, and uncertain outcomes, it’s a good, relieving feeling to know I’ll be going. Next year. Now I just need to hear back from everywhere else so I can start planning the North American tour dates…. More importantly, this means I’ll have ample blog/’job’ security for a few more years…. Click to email (Opens in new window). Share on Facebook (Opens in new window). You a...

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Arse, ‘innit? | Chiral Jones

https://chiraljones.wordpress.com/2010/12/08/arse-innit

Now with hood space! Arse, ‘innit? So, as a scientist, here’s my obligatory post regarding the whole “Arsenic Replacing Phosphorus in DNA Backbone” thing. Whether or not it’s true, it really seems as though Wolfe-Simon. Their case, and that’s a problem. (If you want a full breakdown of why the paper is kind of flawed, check out commentaries by Derek Lowe. In response to criticisms, via Nature News. 8220;We are not going to engage in this sort of discussion,” she wrote in an e-mail to Nature. &#...8221; a...

chiraljones.wordpress.com chiraljones.wordpress.com

Big News | Chiral Jones

https://chiraljones.wordpress.com/2011/01/30/big-news

Now with hood space! Chemjobber does it again! Really, he couldn’t be better at what he does – even if he’s not even specifically trying. Way back when he cross posted. Info about my search for grad schools, I got much more than I bargained for.* An editor of C&EN came across my blog, enjoyed the ‘Chiral Jones Experience,’ and contacted me with interest in picking me up over at CENtral Science. So here are the deets:. Yes, I’ll be blogging for C&EN! Incriminating happy hour pics. I’ll let him intro...

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ACD Labs – Check yo’ internets! | Chiral Jones

https://chiraljones.wordpress.com/2011/02/03/acd-labs-check-yo-internets

Now with hood space! ACD Labs – Check yo’ internets! Just a little something I noticed today while trying to look something up about ACD Labs. This is current as of maybe 20 minutes ago:. Sorry it’s a bit small, I suggest you view the full pic. Check out the first and last entries I’ve included from my screen-capture. Have a chuckle at it before ACD gets wise and fixes it. Either someone at ACD labs has a weird sense of humor, is a dissenter, or there’s some skulduggery afoot from a third party. You are ...

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Jul 17, 2010. Quick and easy flash column fix. Have u just broken the end of your favourite flash column? Is your glassblower over worked and won't get to your column for a few months? Here is a quick and dirty fix for the end of your column. Simply find an appropriately sized disposable nalgene syringe (polypropylene types only, otherwise you will extract out nasty plasticisers, don't use the Terumo ones with the black plunger tips), cut the end off and CAREFULLY (with thick gloves). Jun 11, 2010. As it...

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