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CMMP SQUID Magnetometry

Thursday, August 15, 2013. It's possible to qualitatively study the relaxation of the field in the MPMS without looking at the sample moment. Looking at sample moment as a function of time has significant limitations as the ability to see small changes in field is related to the sample mass and susceptibility, and the ability to see small changes over time is limited to the time it takes to do an extraction through the gradiometer. Monday, March 11, 2013. As discussed in a previous post. Where it was sho...

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CMMP SQUID Magnetometry | squid-cmmp.blogspot.com Reviews
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Thursday, August 15, 2013. It's possible to qualitatively study the relaxation of the field in the MPMS without looking at the sample moment. Looking at sample moment as a function of time has significant limitations as the ability to see small changes in field is related to the sample mass and susceptibility, and the ability to see small changes over time is limited to the time it takes to do an extraction through the gradiometer. Monday, March 11, 2013. As discussed in a previous post. Where it was sho...
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CMMP SQUID Magnetometry | squid-cmmp.blogspot.com Reviews

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Thursday, August 15, 2013. It's possible to qualitatively study the relaxation of the field in the MPMS without looking at the sample moment. Looking at sample moment as a function of time has significant limitations as the ability to see small changes in field is related to the sample mass and susceptibility, and the ability to see small changes over time is limited to the time it takes to do an extraction through the gradiometer. Monday, March 11, 2013. As discussed in a previous post. Where it was sho...

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1

CMMP SQUID Magnetometry: SQUID Extraction Profile Points

http://squid-cmmp.blogspot.com/2011/07/squid-extraction-profile-points.html

Wednesday, July 6, 2011. SQUID Extraction Profile Points. In this graph the uncertainty in moment of a 500 nEMU sample at 30 K and 0 Oe applied field is studied. The extraction distance was set to 4 cm and the moment standard error was measured using the multi-measure function. Multi-measure allows one to place statistical constraints on an ensemble of measurements allowing a certain number to be rejected if they exceed these constraints. Subscribe to: Post Comments (Atom). The Benefits of Multi-Measure.

2

CMMP SQUID Magnetometry: Temperature Control

http://squid-cmmp.blogspot.com/2011/07/temperature-control.html

Wednesday, July 6, 2011. The top graph shows a series of temperature changes with increasingly smaller cooling increments. This illustrates several features of temperature control on cooling. The feature between 0 t 55 minutes is an undercooling. Of the sample tube to get the sample portion. The temperature is then dropped in increments of 10 K, 1 K and 0.1 K. The same general cooling behavior is demonstrated in these cases where undercooling is not applied. One is performing the operation in- but the mo...

3

CMMP SQUID Magnetometry: July 2011

http://squid-cmmp.blogspot.com/2011_07_01_archive.html

Thursday, July 7, 2011. The Benefits of Multi-Measure. The standard MPMS moment measurement averages a specified number of SQUID profiles. This mode of operation is called DC-measure. In the top graph a 14.4 uEMU moment at 0 Oe is measured using a 4 cm scan defined by Np = 24 points. The number of samples is varied and the error in moment is displayed along with 1-sigma error bars. To 40 nEMU which is the performance specification for the moment uncertainty at zero applied field. Since we can only re...

4

CMMP SQUID Magnetometry: Longitudinal Moment Calibration

http://squid-cmmp.blogspot.com/2011/07/longitudinal-calibration.html

Wednesday, July 6, 2011. Calibration of the MPMS SQUID magnetometer is extremely straightforward. There is a calibration factor, the longitudinal calibration factor. That calibrates the moment obtained from the SQUID extraction profile. As long as the SQUID amplifier is appropriately calibrated across its ranges of gain, a single one-point calibration is sufficient. This graph shows M vs. H. There is also a transverse gradiometer. November 22, 2011 at 8:23 PM. Subscribe to: Post Comments (Atom). Very Low...

5

CMMP SQUID Magnetometry: Lost Samples & Sample Mounting Materials

http://squid-cmmp.blogspot.com/2011/06/lost-samples-sample-mounting-materials.html

Friday, June 17, 2011. Lost Samples and Sample Mounting Materials. SQUID samples are generally mounted inside drinking straws using pieces of tape, pieces of straws and capsules to mount the samples themselves. There is an art to this. Losing some sample material is acceptable and part of the learning curve- not telling anyone about it is not! Subscribe to: Post Comments (Atom). Superparamagnetism: ZFC and FC Measurements. Lost Samples and Sample Mounting Materials. 5T MPMS SQUID Magnetometer.

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CMMP Scanning Probe Microscopy: Flattening & Flattening Artifacts

http://spm-cmmp.blogspot.com/2011/06/flattening-flattening-artifacts.html

CMMP Scanning Probe Microscopy. Thursday, June 30, 2011. Flattening and Flattening Artifacts. AFM images generally require some post-processing. One method of post-processing is flattening. In this case a polynomial of order n. Is fit and subtracted from every trace and retrace. It is called "flattening" because this method of processing tends to flatten or unroll an AFM image. It is also a potential source of artifacts. To remedy these artifacts stop bands. Grains on a film surface. In these applica...

sem-cmmp.blogspot.com sem-cmmp.blogspot.com

CMMP Scanning Electron Microscopy: Au coating

http://sem-cmmp.blogspot.com/2013/06/au-coating.html

CMMP Scanning Electron Microscopy. Thursday, June 27, 2013. Generally AuPd is used to coat samples as the metal grains are on the order of 20-25 nm. Given that the JEOL 5900 has a resolution on the order of 20 nm at 30 keV and a 6 mm working distance, such grains would never been seen, though they would certainly be seen in a field emission SEM. The figure above shows the fit of Au film thickness versus sputtering time for a 25 mm target distance and a 30 mA plasma current. The fit is: thickness [nm]...

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CMMP Scanning Probe Microscopy: Magnetic Force Microscopy

http://spm-cmmp.blogspot.com/2011/06/magnetic-force-microscopy.html

CMMP Scanning Probe Microscopy. Monday, June 20, 2011. The force exerted on a dipole is the dot product of the dipole moment and the gradient of the field at the surface. In magnetic force microscopy. MFM- these dipole magnetic forces are detected as a change in cantilever phase and amplitude a finite distance above the surface. In an MFM image, the tip is tapped on the surface. To measure the surface morphology, and then rescanned across the surface 50-150 nm above the surface. Fast MFM in Contact Mode.

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CMMP Ellipsometry: Gaertner Ellipsometer

http://ellip-cmmp.blogspot.com/2011/06/gaertner-ellipsometer.html

Friday, June 17, 2011. The CMMP group at the Florida State University Department of Physics has a Gaertner L116B ellipsometer that is available to the local research community. There are no fees for use of this instrument. Fast; non-contact; cost; ideal for Si oxides and nitrides; ideal for materials with well known optical properties for HeNe visible radiation. Subscribe to: Post Comments (Atom). View my complete profile. CMMP Scanning Electron Microscopy. CMMP Scanning Probe Microscopy.

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CMMP Magneto-Transport

http://mt-cmmp.blogspot.com/2013/10/these-are-optical-photos-of-ppms.html

Friday, October 25, 2013. These are optical photos of the PPMS resistivity pucks. The CMMP group has three of these so that samples can be contacted while one is in the system. Each puck has three stations that include four contacts for transport measurements. These contacts can be accessed either by our break-out box or the PPMS controller's resistivity bridge depending upon the application. Contacting samples is an art, and CMMP will not do that for you. The availability of three sets of contacts, labe...

overview-cmmp.blogspot.com overview-cmmp.blogspot.com

CMMP User Facilities: October 2014

http://overview-cmmp.blogspot.com/2014_10_01_archive.html

Wednesday, October 1, 2014. Because of staffing limitations at the CMMP facility, services requiring CMMP staff may involve some delay as instruments and staff time become available. In general, services are provided on a first-come, first server basis. This rule is subject to the discretion of the facility manager according to the availability of instrumentation, staffing, etc. The entries in italics. Are set as high priority, and the projects in red. Are either currently underway or scheduled.

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CMMP Scanning Probe Microscopy: Tapping AFM: Arabidopsis haliana Grana Membranes

http://spm-cmmp.blogspot.com/2014/03/tapping-afm-arabidopsis-haliana-grana.html

CMMP Scanning Probe Microscopy. Wednesday, March 19, 2014. Tapping AFM: Arabidopsis haliana Grana Membranes. Images of Arabidopsis thaliana. Grana membranes using tapping AFM with the Dimension 3000 AFM. Silicon tapping cantilevers were used, (Olympus. OMCLAC160TS-W2, with 7 nm tip radius and. 42 N/m spring constant), and imaging was performed in air. Grana membranes were isolated through treatment with 2%. Subscribe to: Post Comments (Atom). Tapping AFM: Arabidopsis haliana Grana Membranes.

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CMMP Scanning Electron Microscopy: EDS Detector Window Absorption

http://sem-cmmp.blogspot.com/2012/04/eds-detector-window-absorption.html

CMMP Scanning Electron Microscopy. Thursday, April 12, 2012. EDS Detector Window Absorption. This graph shows the transmission through several different EDS detector windows. The solid line is for the Moxtek AP1.3, the dot-dashed line for the Moxtek HT2.2 and the dashed line for the Moxtek AP3.3. Our EDS detector has an AP3.3 window. The graph is borrowed from F. Scholze and M. Procop, X-Ray Spectrom. Subscribe to: Post Comments (Atom). Beam Energy and Topography: SE1 and SE2. Kaersutite: Low Energy EDS.

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CMMP Scanning Electron Microscopy: Dynamic Focus Correction

http://sem-cmmp.blogspot.com/2012/05/dynamic-focus-correction.html

CMMP Scanning Electron Microscopy. Monday, May 7, 2012. The last image shows the same grid at the same tilt and working distance with dynamic focus correction. On Dynamic focus correction allows the SEM objective lens to have a sweep dependent focal length. Since tilting is always in the Y-direction, this focal length dependence is linked to the Y-deflection amplifier. The image shows about 14 mm of the surface in focus, corresponding to a height difference of 13 mm across the length of the sample.

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CMMP SQUID Magnetometry

Thursday, August 15, 2013. It's possible to qualitatively study the relaxation of the field in the MPMS without looking at the sample moment. Looking at sample moment as a function of time has significant limitations as the ability to see small changes in field is related to the sample mass and susceptibility, and the ability to see small changes over time is limited to the time it takes to do an extraction through the gradiometer. Monday, March 11, 2013. As discussed in a previous post. Where it was sho...

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